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Analysis of selected pharmaceutical compounds and endocrine disruptors in municipal wastewater using solid phase microextraction and gas chromatography

Antoniou Chrysoula V., Koukouraki Elisavet, Diamantopoulos Evaggelos

Απλή Εγγραφή


URIhttp://purl.tuc.gr/dl/dias/41581717-7CC0-4609-9E15-45EF71CF055B-
Αναγνωριστικόhttps://doi.org/10.2175/106143008X390834-
Αναγνωριστικόhttps://www.jstor.org/stable/40575412?seq=1#page_scan_tab_contents-
Γλώσσαen-
Μέγεθος6 pagesen
ΤίτλοςAnalysis of selected pharmaceutical compounds and endocrine disruptors in municipal wastewater using solid phase microextraction and gas chromatographyen
ΔημιουργόςAntoniou Chrysoula V.en
ΔημιουργόςKoukouraki Elisaveten
ΔημιουργόςΚουκουρακη Ελισαβετel
ΔημιουργόςDiamantopoulos Evaggelosen
ΔημιουργόςΔιαμαντοπουλος Ευαγγελοςel
ΕκδότηςWater Environment Federationen
ΠερίληψηThe aim of this work was to develop a simple analytical method to determine the presence of selected pharmaceutical compounds, personal care products, and endocrine disruptors in wastewater treatment plant effluents. In this study, solid-phase microextraction (SPME) and gas chromatography with mass spectroscopy (GC-MS) were used to identify triclosan; 2,4-dichloro phenol; 2,3,4-trichloro phenol; galaxolide; tonalide; estrone; 17-β-estradiol; 17-α-ethinyl estradiol; clofibric acid; and carbamazepine. Extraction parameters such as types of SPME fiber, effect of ionic strength, magnetic stirring, pH, extraction temperature, extraction time, and desorption time were investigated to optimize the SPME-GC method. Also, analytical parameters such as repeatability, linearity, and detection limits were evaluated. The method developed in this study was fast (extraction procedure and GC-MS analysis was around 100 minutes), solvent-free, and low cost. This method was used as a screening test to determine if pharmaceutical compounds, personal care products, and endocrine disruptors were present in wastewater treatment plant effluents samples from the Chania Municipal Wastewater Treatment Plant in Crete, Greece.en
ΤύποςPeer-Reviewed Journal Publicationen
ΤύποςΔημοσίευση σε Περιοδικό με Κριτέςel
Άδεια Χρήσηςhttp://creativecommons.org/licenses/by/4.0/en
Ημερομηνία2015-11-15-
Ημερομηνία Δημοσίευσης2009-
Θεματική ΚατηγορίαGas-liquid chromatographyen
Θεματική ΚατηγορίαGLC (Chromatographic analysis)en
Θεματική ΚατηγορίαVapor-phase chromatographyen
Θεματική Κατηγορίαgas chromatographyen
Θεματική Κατηγορίαgas liquid chromatographyen
Θεματική Κατηγορίαglc chromatographic analysisen
Θεματική Κατηγορίαvapor phase chromatographyen
Βιβλιογραφική ΑναφοράC. V. Antoniou, E. E. Koukouraki and E. Diamadopoulos, “Analysis of selected pharmaceutical compounds and endocrine disruptors in municipal wastewater using solid phase microextraction and gas chromatography," Water Environ. Res., vol.81, no. 7, pp. 664-669, July 2009. doi: 10.2175/106143008X390834en

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